Investigation on the formation of Cu-Fe nano crystalline super-saturated solid solution developed by mechanical alloying

Simple item page
dc.citation.epage388en_US
dc.citation.spage380en_US
dc.citation.volumeNumber550en_US
dc.contributor.authorMojtahedi, M.en_US
dc.contributor.authorGoodarzi, M.en_US
dc.contributor.authorAboutalebi, M.R.en_US
dc.contributor.authorGhaffari, M.en_US
dc.contributor.authorSoleimanian V.en_US
dc.date.accessioned2016-02-08T09:40:41Z
dc.date.available2016-02-08T09:40:41Z
dc.date.issued2013en_US
dc.departmentDepartment of Electrical and Electronics Engineeringen_US
dc.departmentInstitute of Materials Science and Nanotechnology (UNAM)en_US
dc.description.abstractIn this study, the formation of super saturated solid solution in the binary Cu-Fe system was investigated. Three powder blends with 30, 50 and 70 wt.% of Fe were milled for different times to 96 h. The variations of lattice parameter and inter-planar spacing were calculated and analyzed using X-ray diffraction analysis (XDA). The anisotropy of lattice deformation in the FCC phase was studied and the obtained results were compared to milled pure Cu powder. Furthermore, crystallite size was calculated using Scherer formula in comparison with Rietveld full profile refinement method. Considering the previous studies about the formation of non-equilibrium FCC and BCC phases, the phase evolution has been discussed and the proportion of each phase was calculated using Rietveld refinement method. Supplementary studies on the evolution of microstructure and formation of solid solution were carried out using high resolution transmission electron microscopy (HRTEM). Finally, high angle annular dark field (HAADF) imaging was utilized to find out the level of homogeneity in the resulting phases. While true alloying takes place in each phase, the final structure consists of both FCC and BCC nano-crystallites. © 2012 Elsevier B.V. All rights reserved.en_US
dc.identifier.doi10.1016/j.jallcom.2012.10.112en_US
dc.identifier.issn0925-8388
dc.identifier.urihttp://hdl.handle.net/11693/21074
dc.language.isoEnglishen_US
dc.relation.isversionofhttp://dx.doi.org/10.1016/j.jallcom.2012.http://dx.doi.org/10.112en_US
dc.source.titleJournal of Alloys and Compoundsen_US
dc.subjectHAADFen_US
dc.subjectHRTEMen_US
dc.subjectMechanical alloyingen_US
dc.subjectRietveld refinementen_US
dc.subjectSolid solubility extensionen_US
dc.subjectXDAen_US
dc.subjectBcc phasisen_US
dc.subjectCu powdersen_US
dc.subjectFCC phaseen_US
dc.subjectHAADFen_US
dc.subjectHigh-angle annular dark fieldsen_US
dc.subjectHRTEMen_US
dc.subjectInterplanar spacingsen_US
dc.subjectLattice deformationen_US
dc.subjectNanocrystallinesen_US
dc.subjectNon equilibriumen_US
dc.subjectPhase evolutionsen_US
dc.subjectPowder blendsen_US
dc.subjectRefinement methodsen_US
dc.subjectRietvelden_US
dc.subjectRietveld refinement methoden_US
dc.subjectSolid solubility extensionen_US
dc.subjectSupersaturated solid solutionsen_US
dc.subjectXDAen_US
dc.subjectCrystal structureen_US
dc.subjectHigh resolution transmission electron microscopyen_US
dc.subjectMechanical alloyingen_US
dc.subjectMicrostructural evolutionen_US
dc.subjectSolid solutionsen_US
dc.subjectX ray diffraction analysisen_US
dc.subjectRietveld refinementen_US
dc.titleInvestigation on the formation of Cu-Fe nano crystalline super-saturated solid solution developed by mechanical alloyingen_US
dc.typeArticleen_US

Files

Original bundle
Now showing 1 - 1 of 1
Thumbnail Image
Name:
Investigation on the formation of Cu–Fe nano crystalline super-saturated solid solution developed by mechanical alloying.pdf
Size:
1.64 MB
Format:
Adobe Portable Document Format
Description:
Full printable version
Download

Collections

Department of Electrical and Electronics Engineering
Institute of Materials Science and Nanotechnology (UNAM)