Browsing by Subject "Mechanical characteristics"

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Open Access
Mechanical characterization of particulated FRP composite pipes: A comprehensive experimental study
(Elsevier, 2020-12-04) Saghir, F.; Gohari, S.; Mozafari, Farzin; Moslemi, N.; Burvill, C.; Smith, A.; Lucas, S.
Particulated fiber reinforced polymer (FRP) composite pipes encompass unidirectional continuous glass fibers (hoop glass), resin (thermoset polymer vinylester) matrix, chop glass (discontinuous short fibers), and particulate reinforcement (sand) impregnated into resin. They are categorized based on their nominal diameter, pressure class, and stiffness class. Mechanical characteristics of this class of composite materials have not, to date, been comprehensively studied. As such, this paper presents a systematic approach toward comprehensive experimental investigation into their mechanical characterizations in terms of the axial and hoop tensile strengths. The particulated FRP composite pipes used in the current study have glass fibers reinforced along the hoop direction at approximately 89° angle. To assure the experimental data accuracy and reliability, three batches associated with each pipe category were selected which slightly differ in the composition of their constituents. Three specimens per batch were selected and two types of tests were conducted on each specimen. 18 tests (2 × 3 batches × 3 specimens)) were conducted per pipe category (9 tests for hoop and 9 tests for axial). Therefore, 648 tests were conducted in total on 36 pipe categories. Instron 5569A and Instron 8801 universal testing machines were utilized for the axial tensile tests and a split disc hydraulic testing machine for the hoop tensile tests. The mean tensile and the hoop axial stresses and their associated standard deviations were calculated based on the Population Standard Deviation (PSD) equation and then plotted against the material constituents. The results demonstrated that an increase in the composition of particulate reinforcement results in a decrease in the axial and the hoop tensile strengths. However, increasing the ratio of resin, chop glass, and glass fibers contributes to the enhancement of the axial and the hoop tensile strengths. This study provides comprehensive design guidelines for engineers and manufacturing industries.
Open Access
X-ray photoelectron spectroscopy for identification of morphological defects and disorders in graphene devices
(AIP Publishing, 2016) Aydogan, P.; Polat, E. O.; Kocabas, C.; Süzer, Şefik
The progress in the development of graphene devices is promising, and they are now considered as an option for the current Si-based electronics. However, the structural defects in graphene may strongly influence the local electronic and mechanical characteristics. Although there are well-established analytical characterization methods to analyze the chemical and physical parameters of this material, they remain incapable of fully understanding of the morphological disorders. In this study, x-ray photoelectron spectroscopy (XPS) with an external voltage bias across the sample is used for the characterization of morphological defects in large area of a few layers graphene in a chemically specific fashion. For the XPS measurements, an external +6 V bias applied between the two electrodes and areal analysis for three different elements, C1s, O1s, and Au4f, were performed. By monitoring the variations of the binding energy, the authors extract the voltage variations in the graphene layer which reveal information about the structural defects, cracks, impurities, and oxidation levels in graphene layer which are created purposely or not. Raman spectroscopy was also utilized to confirm some of the findings. This methodology the authors offer is simple but provides promising chemically specific electrical and morphological information.