Browsing by Author "Ortac, Bülend"

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Open Access
A bean-like formation of germanium nanoparticles inside CNTs by the subsequent operation of colloidal synthesis and catalytic chemical vapor deposition methods
(Wiley, 2018) Karatutlu, Ali; Boi, F. S.; Wilson, R. M.; Ersoy, O.; Ortac, Bülend; Sapelkin, A.
The first attempts of implanting Ge nanoparticles (Ge NPs) inside iron filled CNTs (IF-CNTs) by a subsequent use of the bench top colloidal synthesis and chemical vapor deposition (CVD) approach is shown. Ge NPs are colloidally synthesized (with a 3.8 ± 0.6 nm in size) before the deposition. The hybrid Ge NPs/IF-CNTs structure and morphology are characterized using high-resolution transmission electron microscopy, scanning electron microscopy, selective area electron diffraction, and X-ray diffraction studies. After the deposition, Ge NPs appear to be grown in size and to be sprinkled almost homogeneously into the IF-CNTs similar to a bean-like deposition. CNTs diameter is also identified to be enlarged drastically when using Ge NPs as a catalyst in CVD compared to the CNTs formation without Ge NPs. In addition, micro-length rectangular Ge µPs are also found outside the nanotube core. Rietveld analysis shows the presence of γ-Fe (Fm-3m), ferromagnetic α-Fe (Im-3m), Fe3C, Ge (Fd-3m), and multiwall CNTs. The results indicate that Ge NPs and IF-CNTs demonstrate cocatalytic activity in increasing the respective sizes, which are dramatically larger than those obtained by the conventional approaches.
Open Access
Femtosecond laser fabrication of fiber based optofluidic platform for flow cytometry applications
(SPIE, 2017) Serhatlioglu, Murat; Elbuken, Çağlar; Ortac, Bülend; Solmaz, Mehmet E.
Miniaturized optofluidic platforms play an important role in bio-analysis, detection and diagnostic applications. The advantages of such miniaturized devices are extremely low sample requirement, low cost development and rapid analysis capabilities. Fused silica is advantageous for optofluidic systems due to properties such as being chemically inert, mechanically stable, and optically transparent to a wide spectrum of light. As a three dimensional manufacturing method, femtosecond laser scanning followed by chemical etching shows great potential to fabricate glass based optofluidic chips. In this study, we demonstrate fabrication of all-fiber based, optofluidic flow cytometer in fused silica glass by femtosecond laser machining. 3D particle focusing was achieved through a straightforward planar chip design with two separately fabricated fused silica glass slides thermally bonded together. Bioparticles in a fluid stream encounter with optical interrogation region specifically designed to allocate 405nm single mode fiber laser source and two multi-mode collection fibers for forward scattering (FSC) and side scattering (SSC) signals detection. Detected signal data collected with oscilloscope and post processed with MATLAB script file. We were able to count number of events over 4000events/sec, and achieve size distribution for 5.95μm monodisperse polystyrene beads using FSC and SSC signals. Our platform shows promise for optical and fluidic miniaturization of flow cytometry systems. © 2017 SPIE.
Open Access
Properties of a microjoule-class fiber oscillator mode-locked with a SESAM
(IEEE, 2011) Lecaplain, C.; Ortac, Bülend; MacHinet G.; Boullet J.; Baumgartl, M.; Schreiber, T.; Cormier, E.; Hideur, A.
Energy scaling of ultrafast Yb-doped fiber oscillators has experienced rapid progress largely driven by many applications that require high average power femtosecond pulses. The fundamental challenge for ultrafast fiber lasers relies on the control of excessive nonlinearity, which limits pulse energy. The development of all-normal dispersion laser cavities based on large-mode-area photonic crystal fibers (PCFs) has enabled significant energy scaling [1-3]. In particular, up to microjoule energy levels have been achieved from rod-type fiber-based oscillators [2-3]. In such lasers, pulse shaping is dominated by the strength of the mode-locking mechanism which determines the pulse properties. In this contribution, we report the generation of high-energy sub-picosecond pulses from a highly normal dispersion fiber laser featuring an Yb-doped rod-type PCF and a large-mode-area PCF [Fig.1(a)]. Passive mode-locking is achieved using saturable absorber mirrors (SAMs). We study the influence of the SAM parameters on performances obtained in this new class of fiber oscillators. The structures exhibit 20 % modulation depths and 500 fs relaxation time with resonant and antiresonant designs. The antiresonant SAM structures ensure absorption bandwidths 45 nm while the resonant structures exhibit 20 nm bandwidths. Stable mode locking with average powers as high as 15 μW at 15 MHz repetition rate, corresponding to microjoule energy level are obtained with all the structures. However, pulse properties and pulse shaping mechanism distinguish between resonant and antiresonant designs. Using a broadband antiresonant SAM leads to generation of highly-chirped pulses with 30 ps duration and 10 nm spectral width [Fig.1(b)]. The output pulses are extra-cavity dechirped down to 550 fs duration. By increasing the strength of the mode-locking mechanism through the combination of the SAM with the NPE process, we obtain shorter pulses with slightly boarder spectra. Indeed, the output pulse duration is decreased from 30 ps to 13 ps by adjusting the wave-plates settings. The dechirped pulse duration is then shortened to 450 fs. We note that the current laser performances are limited to 1 J by the available pump power. Using a resonant SAM structure, the output pulse duration is decreased to 7 ps [Fig.1(b)]. This pulse shortening results from the spectral filtering induced by the limited SAM bandwidth. All these results are in good agreement with numerical simulations which will be discussed in this communication. © 2011 IEEE.